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Dual-layer N-glycoproteomics enhances resolution of serum glycosylation signatures in type 2 diabetes mellitus complicated with coronary heart disease - PubMed

3 hours ago
  • #Coronary heart disease
  • #Type 2 diabetes
  • #N-glycoproteomics
  • Development of an integrated dual-layer N-glycoproteomic strategy combining high-coverage site-specific N-glycosylation profiling with intact N-glycopeptide analysis.
  • Application to serum samples from healthy controls, T2DM, CHD, and T2DM&CHD patients, identifying 497 N-glycosites from 781 site-specific N-glycopeptides and 133 N-glycosites from 341 intact N-glycopeptides.
  • Revealed extensive glycoproteome remodeling in T2DM&CHD, characterized by increased microheterogeneity due to altered sialylation and fucosylation.
  • Site-specific changes in apolipoprotein B (N185, N1523, N2239, N3411) showed stage-dependent patterns linked to lipid dysregulation and vascular injury.
  • Functional enrichment suggests T2DM amplifies inflammation-related glycosylation disturbances predisposing to cardiovascular complications.
  • Correlation with glycosyltransferase expression highlights regulatory relevance of glycan biosynthesis.
  • Provides a mechanistic resource for biomarker discovery in metabolic-cardiovascular comorbidity.